The TGA body weight modify curve is demonstrated in Figure one. The first fat reduction step is definitely the volatilization followed by a major decomposition action. The derivative of weight improve curve in environmentally friendly demonstrates a peak where by the height max is at 427.seventy one ˚C. The MS info is collected all through the entire TGA experiment. Ion currents and TGA mass decline are plotted to be a purpose of temperature (see Figure two). It is crucial to keep in mind that the products and solutions of the TGA examination are normally decomposition products and solutions, and that's genuine in these experiments also. Consequently, the aim is to know the thermal degradation products and solutions of nylon 66. TGA-MS repeatedly monitors the decomposition off gases as being a purpose of time and temperature. The degradation system of the polymer molecules breaking within the C-N bond creates lesser polymer molecules While using the similar device of bicarbonyl polymethylene fragments along with the fragments will stop working into carbon dioxide, carbon monoxide, h2o, and hydrocarbons [five].

TGA-MS provides A fast study on volatiles and decomposition process to identify smaller molecules and particular ion fragments. TGA-FTIR is the best technique to establish specific purposeful teams. TGA-GC/MS permits the separation of a mixture of molecules that often evolve simultaneously in the course of decompositions. Combining distinct techniques together will help comprehend the thermal degradation of products better and uncover the chemical buildings of your off-fuel solutions.

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The GC/MS chromatogram is presented in Determine eight with 6 peaks indicating 6 attainable molecules. At the height max of each labeled peak, There may be an linked mass spectrum and it is plotted in Figure nine. The connected MS spectrum provides a particular structure of a single molecule. This delivers extra exact library search results when compared to TGA-MS. Each MS spectrum in Determine 9 is supplied with a very best matched chemical structure from your library. The constructions attained with the GC/MS experiment agree incredibly perfectly While using the TGA-MS and TGA-FTIR outcomes with an additional chemical separation on the specified temperature.

TGA-FTIR consistently displays the decomposition off gases being a operate of your time and temperature, though GC/MS can independent the several off-gas items that occur off at one place in time.

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